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Optimizing Ethanol Recovery in Winterized Botanical Extracts with Heidolph AUTOaccurate Technology

Optimizing Ethanol Recovery in Winterized Botanical Extracts with Heidolph AUTOaccurate Technology

Ethanol recovered from a winterized batch of botanical extract can be reused for multiple cycles of extraction and winterization. However, due to the dynamic nature of batch evaporation, ensuring a highly productive workflow and high-quality results without residual ethanol requires precise and frequent adjustments to vacuum settings during separation. For less experienced operators, identifying and maintaining optimal parameter settings can be a significant challenge. Striking a balance between effective separation and operational efficiency often demands expertise and constant oversight.

Automated Process Control: Addressing Industry Challenges

Many manufacturers respond to these operational demands by dedicating personnel solely to monitor evaporators and manually adjust vacuum settings. However, this approach often results in inefficiencies, as these technicians may lack sufficient experience with evaporator systems, thereby reducing daily output and operational cost-effectiveness.

To address this challenge, Heidolph has developed the Hei-VAP Industrial packages, which offer an advanced solution to streamline the evaporation process. The innovative AUTOaccurate function automates the detection, adjustment, and maintenance of optimal vacuum settings throughout the evaporation process. By doing so, it eliminates the need for constant manual monitoring. AUTOaccurate ensures that the condenser operates at peak efficiency and further lowers the vacuum to a predefined final pressure after solvent evaporation, enabling the production of high-quality botanical extracts with no residual ethanol.

  Hei-VAP Package: Hei-VAP Industrial with Glassware A1C

Fig 1: Hei-VAP Package: Hei-VAP Industrial with glassware A1C

Ethanol as the Solvent of Choice

Ethanol is widely regarded as an ideal solvent for extraction and winterization processes due to its low toxicity and ease of handling compared to alternative solvents. However, ethanol’s cost, often elevated by taxation, makes its recycling and reuse critical to minimizing production expenses and reducing the environmentalfootprint of manufacturing operations. The automation provided by Heidolph's AUTOaccurate function ensures high-performance distillation, significantly enhancing solvent recovery efficiency and product quality.

Method: Ethanol Recovery with AUTOaccurate

For the batch ethanol recovery from winterized botanical extracts, the Heidolph Hei-VAP Industrial package was employed, leveraging the AUTOaccurate function to achieve optimal results. The operational parameters were set as follows:

  • Recirculating chiller:

    5 °C
  • Heatingbathtemperature:

    60°C
  • Rotation speed:

    130 rpm
  • DeltaT(temperature differential):

    5 °C
  • Final pressure: :

    30 mbar
HEI-VAP Performance Plus Package

Fig 2: HEI-VAP Performance Plus Packages

Results

The process delivered exceptional results, producing a clear, colorless ethanol distillate ready for reuse in extraction and winterization. The botanical extract obtained was clear, golden-colored, and free from solvent residue, ensuring both product quality and compliance with manufacturing standards.

Conclusion

This case study demonstrates how Heidolph’s advanced solutions, specifically the AUTOaccurate function, optimize ethanol recovery for winterized botanical extracts. Compared to manual evaporation methods, AUTOaccurate ensures efficient, automated processes that save time, reduce operational complexity, and produce high-quality extracts. Heidolph’s innovative approach empowers manufacturers to achieve superior results with minimal effort, making it an essential tool for modern botanical processing operations.

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